Chemical anchorage of Hydroxyapatite on 316LSS using a ZrO2 interlayer for orthopedic prosthesis applications
Vol. 25 No. 3 (2012), Research Papers
Vol. 25 No. 3 (2012)

Chemical anchorage of Hydroxyapatite on 316LSS using a ZrO2 interlayer for orthopedic prosthesis applications

Research Papers
Published 2012-09-15
B. Bermúdez Reyes
Instituto de Investigaciones Metalúrgicas, Universidad Michoacana de San Nicolás de Hidalgo. Facultad de Ingeniería Mecánica y Eléctrica, Universidad Autónoma de Nuevo León.
M. E. Contreras García
Instituto de Investigaciones Metalúrgicas, Universidad Michoacana de San Nicolás de Hidalgo
J. L. Almaral Sánchez
Universidad Autónoma de Sinaloa
I. Espitia Cabrera
Facultad de Ingeniería Química, Universidad Michoacana de San Nicolás de Hidalgo
F. J. Espinoza Beltrán
Centro de Investigación y de Estudios Avanzados del I.P.N., Unidad Querétaro
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Keywords

Hydroxyapatite
Zirconia
Biomaterials
Bilayer coating system

How to Cite

Bermúdez Reyes, B., Contreras García, M. E., Almaral Sánchez, J. L., Espitia Cabrera, I., & Espinoza Beltrán, F. J. (2012). Chemical anchorage of Hydroxyapatite on 316LSS using a ZrO2 interlayer for orthopedic prosthesis applications. Superficies Y Vacío, 25(3), 150-156. Retrieved from https://superficiesyvacio.smctsm.org.mx/index.php/SyV/article/view/196
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Abstract

The aim of this work is the study of the interaction mechanisms between hydroxyapatite–zirconia interface and the zirconia layer (ZrO2) on a stainless steel substrate in the HA/ZrO2/316LSS system. The Hydroxyapatite (HA) layer was applied by the screen printing technique on ZrO2 film previously deposited by electrophoresis on 316LSS substrates. The bilayer system was thermally annealed at temperatures less than or equal to 700 °C for a maximum time of 5 minutes. The electro-deposited amorphous layers of zirconium hydroxide with a thickness about  8 µm showed good adherence to the stainless steel substrates and allowed good chemical anchorage with the HA layer after the thermal treatment, producing a thin layer of zirconia stabilized in tetragonal and monoclinic mixed phases. The thermal treatment also degraded HA layer to form calcium phosphates. The bilayer system of HA/ZrO2 on 316LSS substrate ensures a good anchorage, being a good and inexpensive candidate for a protective coating in stainless steel orthopedic prostheses. This solves the low adherence between HA and 316LSS, in addition of the low cost the 316LSS prostheses as a biocompatible system with low production costs.

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